Nanocharacterization Techniques
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Nanocharacterization of Cementitious Composites
This book offers a systemic introduction and summarization of nanoscale characterization techniques on cementitious materials. Cementitious composites are ubiquitous in the realm of construction, serving as the backbone of infrastructure worldwide. These materials, typically composed of cement, aggregates, and water, exhibit a complex interplay of mechanical, chemical, and physical properties. In the introductory chapter, we delve into the fundamental aspects of cementitious composites, exploring their composition, structure, and significance in the construction industry. In the second chapter, we introduced the advancements and applications of nano-characterization techniques for cementitious materials including nanoindentation, nanoscratch, modulus mapping, atomic force microscopy-based nanomechanical mapping techniques. Therefore, in the third chapter, the cementitious materials sample surface processing procedure was introduced. In the fourth chapter, nanoindentation, modulus mapping and PeakForce quantitative nanomechanical mapping (PeakForce QNM) test results were comparatively analysed. In chapter five and six, the nanoscale mechanical properties of sodium aluminosilicate hydrate (N-A-S-H) gel in geopolymer paste with and without nanoparticles was evaluated by grid nanoindentation tests. The nano/micromechanical properties of interfacial transition zones in ordinary concrete, recycled aggregate concrete and geopolymer concrete were investigated in chapter seven, eight and nine. Modelled aggregate samples were used to improve efficiency and reduce unnecessary workload in the microscopic characterization. Finally, challenges and future directions were discussed in chapter ten from cementitious sample surface preparation methods, microscopic characterization method for cementitious materials and testing strategies for complicated interfacial transition zones.
Nanocharacterization Techniques
Author: Osvaldo de Oliveira Jr
language: en
Publisher: William Andrew
Release Date: 2017-03-18
Nanocharacterization Techniques covers the main characterization techniques used in nanomaterials and nanostructures. The chapters focus on the fundamental aspects of characterization techniques and their distinctive approaches. Significant advances that have taken place over recent years in refining techniques are covered, and the mathematical foundations needed to use the techniques are also explained in detail. This book is an important reference for materials scientists and engineers looking for a through analysis of nanocharacterization techniques in order to establish which is best for their needs. - Includes a detailed analysis of different nanocharacterization techniques, allowing readers to explore which one is best for their particular needs - Provides examples of how each characterization technique has been used, giving readers a greater understanding of how each technique can be profitably used - Covers the mathematical background needed to utilize each of these techniques to their best effect, meaning that readers can gain a full understanding of the theoretical principles behind each technique covered - Serves as an important, go-to reference for materials scientists and engineers
Characterization Techniques for Nanomaterials
Manipulation of matter at the nanoscale level is the key factor in nanotechnology, and it is considered as a great driving force behind the current industrial revolution since it offers facile and feasible remedies for many problems. Because of the unique characteristic properties of nanomaterials, they can be employed in a wide variety of fields such as agriculture and food technology, catalysis, biomedical applications, tissue culture engineering, and fertilizers. In this regard, characterization of nanomaterials plays a significant role in determining their optical, thermal, and physicochemical properties. Many techniques have been used in nanomaterial characterization, and the most important techniques are discussed in detail in this book with their principles, basic operation procedures, and applications with suitable examples. In summary, this book offers broad content on the most important chemical and structural characterization techniques of nanomaterials. The book offers comprehensive coverage of the most essential topics, including the following: Provides a comprehensive understanding of physical and chemical characterization techniques of nanomaterials Includes details about basic principles of each characterization technique with appropriate examples Covers most of the important characterization techniques that should be known to undergraduate/early career scientists/beginners in materials chemistry Provides all the basic knowledge to understand and carry out the respective analysis of nanomaterials Fulfills the timely need of a book that covers the most important and useful characterization techniques in nanomaterial characterization Up to date, there are no other books/book chapters which discuss most of these nanocharacterization techniques in one segment with all the basic instrumentation details and narrated examples of nanomaterial characterization. In a nutshell, this book will be a great asset to undergraduates/early career scientists/beginners of material science as it provides a comprehensive and complete understanding of most of the techniques used in nanocharacterization tools in a short time. Intended audience is based on science education while specifically focusing on undergraduates/graduate students/early scientists and beginners of chemistry, materials chemistry, and nanotechnology and nanoscience.