Multiple Detection In Size Exclusion Chromatography

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Multiple Detection in Size-exclusion Chromatography

For four decades, size-exclusion chromatography has played a prominent role in characterizing polymers, by determining the polymer's molar mass averages, often not absolutely but relative to some calibration standard. Not satisfied, scientists now want to determine the absolute molar mass averages and distribution and to characterize their long-chain and short-chain branching, tacticity, copolymer and base-pair sequences, and other matters. Oh yes, and they want all this as a continuous function of the molar mass of the analyte. Fortunately, the technique is endowed with a number of detection methods, and the 18 papers here explain the role of those various detection methods and the synergistic effect of combining them in different configurations to obtain desired results. Distributed in the US by Oxford University Press. Annotation : 2004 Book News, Inc., Portland, OR (booknews.com).
Handbook Of Size Exclusion Chromatography And Related Techniques

Documenting critical advances in this rapidly evolving field, the Second Edition highlights the need for new applications and technologies that assist in the determination of molecular weight and molecular weight distributions of polymers in an accurate, efficient manner. This volume presents the latest findings from a international team of specialists and continues to inspire and extend practical applications of size exclusion chromatography (SEC). It includes six new chapters covering high-speed size exclusion chromatography, SEC of low molecular weight materials, and the extended family of techniques, from two-dimensional liquid chromatography to high osmotic pressure chromatography.
Multidimensional HPLC of Polymers

Author: Harald Pasch
language: en
Publisher: Springer Science & Business Media
Release Date: 2013-06-12
This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers. It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.