Design And Control Of Distillation Systems For Separating Azeotropes
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Design and Control of Distillation Systems for Separating Azeotropes
Author: William L. Luyben
language: en
Publisher: John Wiley & Sons
Release Date: 2011-12-06
Hands-on guidance for the design, control, and operation of azeotropic distillation systems Following this book's step-by-step guidance, readers learn to master tested and proven methods to overcome a major problem in chemical processing: the distillation and separation of azeotropes. Practical in focus, the book fully details the design, control, and operation of azeotropic distillation systems, using rigorous steady-state and dynamic simulation tools. Design and Control of Distillation Systems for Separating Azeotropes is divided into five parts: Fundamentals and tools Separations without adding other components Separations using light entrainer (heterogeneous azeotropic distillation) Separations using heavy entrainer (extractive distillation) Other ways for separating azeotropes The distillation methods presented cover a variety of important industrial chemical systems, including the processing of biofuels. For most of these chemical systems, the authors explain how to achieve economically optimum steady-state designs. Moreover, readers learn how to implement practical control structures that provide effective load rejection to manage disturbances in throughput and feed composition. Trade-offs between steady-state energy savings and dynamic controllability are discussed, helping readers design and implement the distillation system that best meets their particular needs. In addition, economic and dynamic comparisons between alternative methods are presented, including an example of azeotropic distillation versus extractive distillation for the isopropanol/water system. With its focus on practical solutions, Design and Control of Distillation Systems for Separating Azeotropes is ideal for engineers facing a broad range of azeotropic separation problems. Moreover, this book is recommended as a supplemental text for undergraduate and graduate engineering courses in design, control, mass transfer, and bio-processing.
Integrated Process Design and Operational Optimization via Multiparametric Programming
This book presents a comprehensive optimization-based theory and framework that exploits the synergistic interactions and tradeoffs between process design and operational decisions that span different time scales. Conventional methods in the process industry often isolate decision making mechanisms with a hierarchical information flow to achieve tractable problems, risking suboptimal, even infeasible operations. In this book, foundations of a systematic model-based strategy for simultaneous process design, scheduling, and control optimization is detailed to achieve reduced cost and improved energy consumption in process systems. The material covered in this book is well suited for the use of industrial practitioners, academics, and researchers. In Chapter 1, a historical perspective on the milestones in model-based design optimization techniques is presented along with an overview of the state-of-the-art mathematical tools to solve the resulting complex problems. Chapters 2 and 3 discuss two fundamental concepts that are essential for the reader. These concepts are (i) mixed integer dynamic optimization problems and two algorithms to solve this class of optimization problems, and (ii) developing a model based multiparametric programming model predictive control. These tools are used to systematically evaluate the tradeoffs between different time-scale decisions based on a single high-fidelity model, as demonstrated on (i) design and control, (ii) scheduling and control, and (iii) design, scheduling, and control problems. We present illustrative examples on chemical processing units, including continuous stirred tank reactors, distillation columns, and combined heat and power regeneration units, along with discussions of other relevant work in the literature for each class of problems.
Industrial Chemical Separation
Author: Timothy C. Frank
language: en
Publisher: Walter de Gruyter GmbH & Co KG
Release Date: 2023-08-07
A fresh new treatment written by industry insiders, this work gives readers a remarkably clear view into the world of chemical separation. The authors review distillation, extraction, adsorption, crystallization, and the use of membranes – providing historical perspective, explaining key features, and offering insights from personal experience. The book is for engineers and chemists with current or future responsibility for chemical separation on a commercial scale – in its design, operation, or improvement – or for anyone wanting to learn more about chemical separation from an industrial point of view. The result is a compelling survey of popular technologies and the profession, one that brings the art and craft of chemical separation to life. Ever wonder how popular separation technologies came about, how a particular process functions, or how mass transfer units differ from theoretical stages? Or perhaps you want some pointers on how to begin solving a separation problem. You will find clear explanations and valuable insights into these and other aspects of industrial practice in this refreshing new survey.